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Archaeological Glass Corrosion

Can micro chemical spot testing accurately identify composition of glass corrosion?

Presented at ICOM-CC Glass and Ceramic Working Group Interim Meeting and Icon Ceramics and Glass Conference. London, September 2019.

Co-authors:  Marie Desrochers (WUDPAC Class of 2021) and Dr. Rosie Grayburn (Associate Scientist and Lab Manager, Department of Conservation Winterthur Museum)

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Background

Archaeological glass offers unique challenges for analysis because of its complex laminar structure, a degraded surface that is chemically distinct from the bulk glass. This project assessed the viability of microchemical spot testing as a method for analyzing the composition of glass corrosion.

 

"Testing the test" expands our understanding of existing tools and their application.

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Analysis

We  compared results of a spot test for calcium to elemental point analysis and mapping with X-ray fluorescence.

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Conclusion​

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The microchemical spot test for calcium may not be sensitive enough to detect the trace amounts of calcium in archeological glass corrosion.

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